2-Pyridine selenyl bromide

CAS: 91491-61-1

Ref. 3D-FP11022

Produktinformation

• Name: 2-Pyridine selenyl bromide
• Marke: Biosynth
• Beschreibung: 2-Pyridine selenyl bromide is a co-precursor for the synthesis of 2-selenides. It can be prepared by reacting 2-pyridinesulfonyl chloride with sodium periodate in acetonitrile. This compound can then be converted to a 2-selenide by treatment with methanol and periodic acid. The analytical and preparative methods are shown below:Analytical: Dissolve the sample in dichloromethane, add triethylamine, and extract into diethyl ether. Add a small amount of potassium bromide to the organic layer and evaporate to dryness under vacuum. Recrystallize from acetonitrile.Methanolysis: Dissolve the sample in methanol, add a catalytic amount of hydrochloric acid, and heat at reflux for 12 hours. Cool the solution, filter off any insoluble material, evaporate to dryness

Chemische Eigenschaften

• Molekulargewicht: 236.96 g/mol
• Formel: C₅H₄BrNSe
• Reinheit: Min. 95%
• InChl: InChI=1S/C5H4BrNSe/c6-8-5-3-1-2-4-7-5/h1-4H
• InChI Key: InChIKey=HORGYCFLJWJACY-UHFFFAOYSA-N
• SMILES: Br[Se]c1ccccn1