2-Pyridine selenyl bromide

CAS: 91491-61-1

Ref. 3D-FP11022

Información del producto

• Nombre: 2-Pyridine selenyl bromide
• Marca: Biosynth
• Descripción: 2-Pyridine selenyl bromide is a co-precursor for the synthesis of 2-selenides. It can be prepared by reacting 2-pyridinesulfonyl chloride with sodium periodate in acetonitrile. This compound can then be converted to a 2-selenide by treatment with methanol and periodic acid. The analytical and preparative methods are shown below:Analytical: Dissolve the sample in dichloromethane, add triethylamine, and extract into diethyl ether. Add a small amount of potassium bromide to the organic layer and evaporate to dryness under vacuum. Recrystallize from acetonitrile.Methanolysis: Dissolve the sample in methanol, add a catalytic amount of hydrochloric acid, and heat at reflux for 12 hours. Cool the solution, filter off any insoluble material, evaporate to dryness

Propiedades químicas

• Peso molecular: 236.96 g/mol
• Fórmula: C₅H₄BrNSe
• Pureza: Min. 95%
• InChI: InChI=1S/C5H4BrNSe/c6-8-5-3-1-2-4-7-5/h1-4H
• Clave InChI: InChIKey=HORGYCFLJWJACY-UHFFFAOYSA-N
• SMILES: Br[Se]c1ccccn1