3-Formylphenylboronic acid mida ester
CAS: 1257642-72-0
Ref. 3D-HAC64272
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Información del producto
3-Formylphenylboronic acid mida ester is an intermediate in the synthesis of 1,2-diaminocyclohexane. It is synthesized by reductive amination of 3-formylphenylboronic acid and an amine. This reaction proceeds smoothly at room temperature in the presence of a microwave irradiation. The yield of this reaction can be increased using a reducing agent such as formic acid or sodium borohydride.
Formal Synthesis:
1) Add 3-formylphenylboronic acid to a suspension of ammonium chloride in methanol, followed by heating at reflux for 30 minutes
2) After cooling to room temperature, add the amine and heat at reflux for 2 hours
3) After cooling to room temperature, dilute with water and extract with ether
4) Extract the organic layer with water and dry over sodium sulfate
Propiedades químicas
Consulta técnica sobre: 3D-HAC64272 3-Formylphenylboronic acid mida ester
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