
2-Pyridine selenyl bromide
CAS :
Ref. 3D-FP11022

Informations sur le produit
Nom:2-Pyridine selenyl bromide
Marque:Biosynth
Description :2-Pyridine selenyl bromide is a co-precursor for the synthesis of 2-selenides. It can be prepared by reacting 2-pyridinesulfonyl chloride with sodium periodate in acetonitrile. This compound can then be converted to a 2-selenide by treatment with methanol and periodic acid. The analytical and preparative methods are shown below:Analytical: Dissolve the sample in dichloromethane, add triethylamine, and extract into diethyl ether. Add a small amount of potassium bromide to the organic layer and evaporate to dryness under vacuum. Recrystallize from acetonitrile.Methanolysis: Dissolve the sample in methanol, add a catalytic amount of hydrochloric acid, and heat at reflux for 12 hours. Cool the solution, filter off any insoluble material, evaporate to dryness
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Propriétés chimiques
Masse moléculaire :236.96 g/mol
Formule :C5H4BrNSe
Degré de pureté :Min. 95%
InChI :InChI=1S/C5H4BrNSe/c6-8-5-3-1-2-4-7-5/h1-4H
Code InChI :InChIKey=HORGYCFLJWJACY-UHFFFAOYSA-N
SMILES :Br[Se]c1ccccn1