1,3-Dichloro-5-nitrobenzene
CAS: 618-62-2
Ref. 3D-FD139568
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Product Information
- 1,3-Dichloro-5-Nitrobenzene
- 3,5-Dichloro Nitrobenzene
- 3,5-Dichloro-1-nitrobenzene
- 5-Nitro-m-dichlorobenzene
- Benzene, 1,3-dichloro-5-nitro-
- NSC 53841
- NSC 60642
1,3-Dichloro-5-nitrobenzene is a chemical intermediate used in the synthesis of carbamazepine. It is obtained by the desalting of 1,3-dichloro-5-nitrobenzene with water and methanol. The proton resonances are observed at 3.2 ppm and the dipole moment is 2.6 D. The chemical ionization mass spectrum shows a molecular ion peak at m/z (relative abundance) 144 and an isotopic pattern characteristic for C12H10Cl2N2O4+ (100%). The NMR spectrum shows three sets of peaks at δ 6.8, δ 7.4, and δ 8.6 that correspond to the two diastereomers of 1,3-dichloro-5-nitrobenzene:
1)
CH3Cl+CH=CH2 + H+ → CH
Chemical properties
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