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Ethyl 2-(m-Nitrobenzylidene)-acetoacetate
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Ethyl 2-(m-Nitrobenzylidene)-acetoacetate

CAS: 39562-16-8

Ref. 3D-FE32300

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Estimated delivery in United States, on Thursday 18 Jul 2024

Product Information

Name:
Ethyl 2-(m-Nitrobenzylidene)-acetoacetate
Synonyms:
  • Butanoic Acid, 2-[(3-Nitrophenyl)Methylene]-3-Oxo-, Ethyl Ester
  • Cinnamic acid, α-acetyl-m-nitro-, ethyl ester
  • Ethyl 2-(3-nitrobenzylidene)-3-oxobutanoate
  • Ethyl 2-(m-nitrobenzylidene)acetoacetate
  • Ethyl 2-[(3-nitrophenyl)methylene]-3-oxobutanoate
  • Ethyl 3-nitrobenzylideneacetoacetate
  • Ethyl α-acetyl-β-(m-nitrophenyl)acrylate
  • NSC 637307
Description:

Ethyl 2-(m-nitrobenzylidene)-acetoacetate is an organic compound that is used in the synthesis of nitrendipine. It can be prepared by reacting acetoacetate with m-nitrobenzaldehyde in the presence of a catalytic amount of diisopropylammonium chloride. The reaction liquid is evaporated to give high purity product and then it is recrystallized from a suitable solvent. The yield of this reaction is about 60%. Ethyl 2-(m-nitrobenzylidene)-acetoacetate impurities include ethyl benzoate, ethyl 4-nitrobenzoate, ethyl 4-hydroxybenzoate, ethyl 3-hydroxy-4-nitrobenzoate, and ethyl 3,4-dihydroxybenzoate.

Notice:
Our products are intended for lab use only. For any other use, please contact us.
Brand:
Biosynth
Long term storage:
Notes:

Chemical properties

Molecular weight:
263.25 g/mol
Formula:
C13H13NO5
Purity:
Min. 95%
MDL:
Melting point:
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Concentration:
EINECS:
Merck:
HS code:

Hazard Info

UN Number:
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